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1 article(s) from Bondarenko, Lidija

Building complex carbon skeletons with ethynyl[2.2]paracyclophanes

Ina Dix,
Lidija Bondarenko,
Peter G. Jones,
Thomas Oeser and
Henning Hopf

Beilstein J. Org. Chem. 2014, 10, 2013–2020, doi:10.3762/bjoc.10.209

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Graphical Abstract

Scheme 1: Planar and layered ethynyl aromatics as building blocks for extended aromatic structures.

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Scheme 2: Previous coupling experiments with pseudo-ortho-diethynyl[2.2]paracyclophane 4.

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Scheme 3: Glaser coupling of pseudo-gem-diethynyl[2.2]paracyclophane 2.

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Scheme 4: Glaser coupling of pseudo-ortho-diethynyl[2.2]paracyclophane, 4.

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Figure 1: Above: The molecule of compound 11 in the crystal; ellipsoids represent 30% probability levels. Onl...

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Figure 2: Above: The molecule of compound 12 in the crystal; ellipsoids represent 50% probability levels. Onl...

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Scheme 5: Sonogashira coupling of aldehyde 13 with ortho-diiodobenzene (14).

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Scheme 6: Preparation of benzologs of dimers 11/12.

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Figure 3: Above: The molecule of compound 19 in the crystal; ellipsoids represent 50% probability levels. Sol...

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Figure 4: Above: One of the three independent molecules of compound 20 in the crystal; ellipsoids represent 3...

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Scheme 7: Cross dimerization of 1 and 4.

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Figure 5: The molecule of compound 22 in the crystal; ellipsoids represent 50% probability levels.

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Scheme 8: An attempt to prepare a biphenylenophane.

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Figure 6: The molecule of compound 26 in the crystal; ellipsoids represent 50% probability levels.

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Published 27 Aug 2014

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